Problem | Cause | Solution |
There is leak | Teflon joints are loose | Tighten joints |
*Run leak check from Maintenance | Sample heating tube is broken | Replace sample heating tube |
Inlet O-ring is broken or damaged | replace with new O-ring | |
Flowcell has an internal leak |
Disassemble and re-assemble flowcell | |
Sensitivity drop | Calibration is bad | Remake standard and calibrate |
There is leak | Fix the leak (see above) | |
Sample heating tube is faulty | Replace sample heating tube | |
Wrong method selectedr | Change method | |
Incomplete combustion of sample | Change method or reduce sample amount | |
Affected by interference (halogens) | Reduce sample amount or use additive B and/or M | |
Affected by residue on sample boat | Wash or replace sample boat | |
Joints/cell are soileded | Wash or replace them | |
Flow error | Air pump is faulty (2000 hrs lifetime) | Replace with new air pump |
There is leak | Fix the leak (see above) | |
Sample heating tube is plugged | Replace sample heating tube | |
Activated carbon filter is plugged | Replace activated carbon pencil filter | |
Flow sensor is broken | Replace with new flow sensor | |
Plugged V1 valve (flow rate drops during atomize step) |
Replace V1 valve (no harm in trying to clean it first) | |
Strange peak shape / no peak | Affected by interference | Change method or reduce sample amount or use additive |
Maximum H3 temperature is low
(Thermocouple position is not good or SSR/switching power supply is broken) |
Adjust thermocouple position Replace SSR/switching power supply |
|
H3
does not heat up (H3 coil or thermocouple is broken) |
Replace H3 heater coil or thermocouple | |
Mercury collector tube is faulty | Replace mercury collector tube | |
High blank | Sample heating tube is contaminated | Replace to new sample heating tube |
Joints are contaminated | Replace or wash Joints and cell | |
Boat handling poker is contaminated | Replace or wash boat handling poker | |
Sample boat is contaminated | Replace or wash sample boat | |
Humidifier bottle is contaminated | Replace or wash dehumidifier bottle | |
Flowcell is contaminated | Replace or wash cell | |